[关键词]
[摘要]
目的: 优选蒙药狗尾草果实中总鞣质的最佳提取工艺。方法: 采用正交试验法L9( 34 ) 设计该试验,
以狗尾草果实中的总鞣质含量作为考察指标,采用络合滴定法测定含量,考查影响鞣质提取的因素,优化狗尾草
果实中总鞣质的提取方法和条件。结果: 优选工艺为选用12 倍药材量的70%丙酮,超声提取1 h,功率70 W。
结论: 优选工艺提取的总鞣质含量较高,该工艺合理可行。
[Key word]
[Abstract]
Objective: To optimize the extraction conditions for total tannin from Setaria viridis
( L. ) Beauv. ripe fruits. Methods: Orthogonal test was used to screen the optimal the extraction conditions.
The content of total tannin was choosed as the assessment index,compleximetry was used for the
measurement. Results: The best conditions for the extraction process were as followed. The ratio of material
to solution as 1 ∶12,70%acetone solution,extracting for 60 minutes by ultrasonic wave. Conclusion:
The optimum extraction process is reliable with higher extracting ratio of the active components.
[中图分类号]
R284. 2
[基金项目]
收稿日期: 2013-01-11; 修回日期: 2013-05-08
基金项目: 内蒙古自治区自然科学基金( 2010MS1206)
作者简介: 张爱武( 1973-) ,女,内蒙古医科大学附属医院药剂部副主任药师,理学硕士。
通讯作者: 刘乐乐,教授,硕士研究生导师,E-mail: liulele8821@ sina. com 内蒙古医科大学药学院, 010110