[关键词]
[摘要]
?目的: 制订内蒙古产山川柳的质量标准。方法: 采用性状、薄层色谱鉴别进行定性鉴别,用高效液
相色谱法测定内蒙古不同产地的山川柳药材槲皮素含量。结果: 明确了内蒙古山川柳的性状鉴别特征,建立了
以活性成分槲皮素对照的薄层色谱鉴别方法,制订了槲皮素含量不低于0. 4 mg /g 的质量标准。结论: 所建立的
方法简便、专属性高,适用于内蒙古产山川柳药材的质量控制。
[Key word]
[Abstract]
Objective: To establish the quality standards of Chuan Shanliu of Inner Mongolia province.
Methods: TLC and Morphological characters were used for qualitative identification and HPLC
was used for quantitative detection by determining quercetin of medicinal materials from different producing
area. Result: Morphological characters which could be used for the identification were clarified.
A new TLC method using the active component of Chuan Shanliu,quercetin,as the control was established.
The quality standard that the content of quercetin was no less than 0. 4 mg /g was formulated.
Conclusion: The quality standard established in this paper is convenient,peculiar and suitable for the
quality control of Chuan Shanliu of Inner Mongolia province.
[中图分类号]
R917
[基金项目]
?收稿日期: 2012-12-25; 修回日期: 2013-04-15
基金项目: 蒙古口蘑等10 味蒙药材质量标准研究( MX 2005 BZ008)
作者简介: 李怀斌( 1962-) ,男,陕西省咸阳市食品药品检验所副主任中药师。
通讯作者: 乌仁图雅,教授,E-mail:
lhb3166692@163. com 内蒙古医科大学蒙医药学院, 010110